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World Journal of Pharmacy and
Pharmaceutical Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Medical Research and Technology

Impact Factor : 8.025

ICV : 84.65

WJPPS Citation

	All	Since 2019
Citation	5450	3969
h-index	23	20
i10-index	134	84

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WJPPS Rank with Index Copernicus Value 84.65 due to high reputation at International Level

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WJPPS: NOVEMBER ISSUE PUBLISHED

NOVEMBER 2024 Issue has been successfully launched on 1 NOVEMBER 2024.

Abstract

DEVELOPMENT AND VALIDATION OF A RP-HPLC METHOD FOR THE ESTIMATION OF NISOLDIPINE IN PURE AND FORMULATIONS

K. Kamala*, M. Rama Krishna, D. Jeevanmani Babu, M. Nagendra Babu and N. Anil Kumar

ABSTRACT

A simple, precise, rapid and accurate gradient HPLC method has been developed for the estimation of Nisoldipine in bulk and tablet formulations. The chromatographic separation was achieved on Phenomenex C18 (250 mm x 4.6 mm, 5.0 μm) column using the mobile phase composed of acetonitrile : methanol in the ratio of 50:50 (v/v) at a flow rate of 1 mL/min and Nisoldipine was eluted at 3.340 min. Quantification and linearity was achieved at 237 nm within the concentration range of 10-80 μg/ml. The method was validated for specificity, linearity, accuracy, precision, LOD and LOQ as per the ICH guidelines and was found to be suitable to be employed in quality control.

Keywords: RP-HPLC, validation, nisoldipine and tablets.

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