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World Journal of Pharmacy and
Pharmaceutical Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Medical Research and Technology

Impact Factor : 8.025

ICV : 84.65

WJPPS Citation

	All	Since 2019
Citation	5450	3969
h-index	23	20
i10-index	134	84

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WJPPS introducing updated version of OSTS (online submission and tracking system), which have dedicated control panel for both author and reviewer. Using this control panel author can submit manuscript

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WJPPS Impact Factor has been Increased to 8.025 for Year 2024.

WJPPS Rank with Index Copernicus Value 84.65 due to high reputation at International Level

Scope Indexed

WJPPS is indexed in Scope Database based on the recommendation of the Content Selection Committee (CSC).

WJPPS: NOVEMBER ISSUE PUBLISHED

NOVEMBER 2024 Issue has been successfully launched on 1 NOVEMBER 2024.

Abstract

DEVELOPMENT AND VALIDATION OF RP-CATION EXCHANGE CHROMATOGRAPHIC METHOD FOR ESTIMATION OF DIVALENT METALLIC IONS FROM BULK AND PHARMACEUTICAL PRODUCTS

Dileep M. Bhosale*, Anna Pratima G. Nikalje

ABSTRACT

A novel, simple and rapid RP-HPLC method was developed for the simultaneous determination of divalent Zn and Fe in pharmaceutical products. The analysis was carried out on Whatman Partisil 10 SCX (250 x 4.6) mm, 10μm column with 2.0 mL/min isocratic flow rate at 295 nm wavelength and the elution of both the components was established within 15 minutes. The retention times of Zn and Fe were about 8 and 9 minutes respectively. The proposed method was validated as per current ICH guidelines for specificity, linearity, robustness, limit of detection, limit of quantification, precision, recovery and solution stability parameters. The exhaustive method study was performed to indicate the stability indicating nature of method.

Keywords: Divalent metal ions, 1,10- Phenanthroline, Zinc (Zn2+), Iron (Fe2+), Cation Exchange.

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