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World Journal of Pharmacy and
Pharmaceutical Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Medical Research and Technology

Impact Factor : 8.025

ICV : 84.65

WJPPS Citation

	All	Since 2019
Citation	5450	3969
h-index	23	20
i10-index	134	84

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WJPPS Rank with Index Copernicus Value 84.65 due to high reputation at International Level

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WJPPS is indexed in Scope Database based on the recommendation of the Content Selection Committee (CSC).

WJPPS: NOVEMBER ISSUE PUBLISHED

NOVEMBER 2024 Issue has been successfully launched on 1 NOVEMBER 2024.

Abstract

DEVELOPMENT AND VALIDATION OF AN RP-HPLC METHOD FOR ANALYSIS OF CRISABOROLE

Amol Pimpale*, Sheetal Gondkar and Smita Aher

ABSTRACT

A simple, sensitive and accurate RP-HPLC method has been developed for the determination of Crisaborole in bulk formulation. The λmax of the Crisaborole was found to be 241nm in 10 mM Ammonium acetate buffer: ACN [60:40 % v/v]. pH 4.5. The method shows high sensitivity with linearity 5 to 25μg/ml (regression equation: y = 316606x - 427583; r2 = 0.9992). The various parameters according to ICH guidelines and USP are followed for validating and testing of this method. The Detection limit and quantitation limit were found to be 0.1094 μg ml –1 and 0.3316 μg ml–1 respectively. The results demonstrated that the procedure is accurate, specific and reproducible (RSD

Keywords: Crisaborole, HPLC method.

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