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World Journal of Pharmacy and
Pharmaceutical Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Medical Research and Technology

Impact Factor : 8.025

ICV : 84.65

WJPPS Citation

	All	Since 2019
Citation	5450	3969
h-index	23	20
i10-index	134	84

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WJPPS Rank with Index Copernicus Value 84.65 due to high reputation at International Level

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WJPPS: APRIL ISSUE PUBLISHED

April Issue has been successfully launched on 1 April 2024.

Abstract

DEVELOPMENT AND VALIDATION OF REVERSE PHASE HPLC DISSOLUTION METHOD FOR DETERMINATION OF IBANDRONATE SODIUM IN TABLET DOSAGE FORM

Jineetkumar B. Gawad*¹, Pritam S. Jain², Atul A. Shirkhedkar², Sanjay J. Surana²

¹St. John Institute of Pharmacy and Research, Palghar (E), M.S India.

²R. C. Patel Institute of Pharmaceutical Education and Research, Shirpur (M.S.) India.

ABSTRACT

A simple, accurate and sensitive liquid chromatographic method has been developed for the determination of ibandronate sodium drug substance in tablet dosage form. The separation was achieved on Hypersil BDS C18 (250mm X 4.6mm), 5μm column. The mobile phase consisted of Buffer: ACN (95:05) v/v; flow rate 1.0 ml min−1 at ambient temperature. The analytes were monitored by PDA detector. The method was validated for specificity, precision, linearity, solution stability and accuracy. The average recoveries for ibandronate were in the range of 99.0�102.0% and the method can be successfully applied for the routine analysis of ibandronate sodium drug substance.

Keywords: Reverse Phase HPLC, Ibandronate sodium, Stability indicating, Validation.

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